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http://hdl.handle.net/123456789/867
Title: | Process for continuous separation of active principles from vegetable oils using membrane bioreactors | Other Titles: | Procedeu de separare continua a principiilor active din uleiuri vegetale utilizand bireactoare membrane | Authors: | Batrinescu, Gheorghe Cuciureanu, Adriana Popa, Ovidiu Babeanu, Narcisa Elena |
Keywords: | Squalene;Vegetable oils;Membranes;Bioreactor | Issue Date: | 30-Jun-2016 | Abstract: | The invention relates to a process and an installation for separation of active principles from vegetable oils. According to the invention, the process comprises the enzymatic hydrolysis of a vegetable oil mixture having a minimum content of 1 % squalene with an enzymatic solution of lipase obtained from Candida Rugosa and a surfaceactive emulsifying agent in a ratio of 1 :1 as compared with the oil, the resulting mixture being subjected to separation into a fraction rich in glycerine and nonsaponifiable matters and a fraction with high concentration of saponifiable matters and active principles which is further admixed with an extraction solvent, and the homogeneous mixture is subjected to separation, to result in a permeate that mostly contains squalene which is finally purified by distillation, the process stages being performed continuously and automatically. The installation, as claimed by the invention, consists of a subassembly (A) comprising some vegetable oil and enzymatic solution storage vessels (1 and 3), respectively, a hydrolysis reactor (5) and an enzymatic membrane bioreactor (8) provided with hydrophilic affinity ultrafiltration membranes for separating the enzymatic hydrolysis mixture, and a subassembly (B) for fractionation of the mixture of hydrolysis products and squalene which comprises a membrane bioreactor (1 8) provided with hydrophobic affinity ultrafiltration membranes for separating the active principles, a distillation column (20) for advanced squalene purification and some automation units (1 0 and 22) that ensure the continuity of the process stages. |
Description: | Patent Assignee Name(s) and Code(s): ECOIND INST NAT CERC DEZVOLTARE ECOLOGIE |
URI: | http://hdl.handle.net/123456789/867 |
Appears in Collections: | Patents |
Files in This Item:
File | Description | Size | Format | Existing users please |
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Documentatie RO131223A0.pdf | 59.26 kB | Adobe PDF | Request a copy | |
RO131223A0.pdf | 93.67 kB | Adobe PDF | Request a copy | |
Brevet de Inventie Batrinescu Gh..pdf | 1.64 MB | Adobe PDF | Request a copy |
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