Please use this identifier to cite or link to this item: http://hdl.handle.net/123456789/870
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dc.contributor.authorDorobantu, Maria-
dc.contributor.authorZlota, Arie-
dc.contributor.authorBarca, Elena-
dc.date.accessioned2017-04-20T13:46:06Z-
dc.date.available2017-04-20T13:46:06Z-
dc.date.issued1982-11-30-
dc.identifier.otherPatent no. RO 80441-A-
dc.identifier.urihttp://hdl.handle.net/123456789/870-
dc.descriptionPatent Assignee Name(s) and Code(s): COMB PETROCH BORZES; INST EPURAREA APELOR REZen_US
dc.description.abstractPara-­toluene-­sulphonic acid is prepd. by using the residue from di-­p-­tolyl-­trichloroethane prodn. which contains 60% H2SO4 and 27% toluene-­sulphonic acid. The residue is treated with toluene in ratio 1 : 1 to 1 : 4 (1 :1 :8), with stirring and heating, at 84­-140 (110­-114) deg.C. Unreacted­ and excess toluene distil azeotropically with water. After sepg. the water ­toluene layers, the water is discharged from process. Toluene is recirculated. Re-fluxing is continued 5­-24 hrs., when the sulpho-­mass contains 1-­6% H2SO4. After cooling to 50-­100 (70) deg.C, the vacuum distn. of excess toluene is continued. The excess toluene is reused in process. The resulting sulpho-­mass contains 85% p-­toluene-­sulphonic acid.en_US
dc.language.isoen_USen_US
dc.subjectPara-­toluene-­sulphonic aciden_US
dc.subjectPreparationen_US
dc.titlePara-­toluene-­sulphonic acid prepn. ­ by treating di:para-­tolyl­-tri:chloro­ethane prodn. residue, contg. sulphuric acid and toluene­-sulphonic acid, with tolueneen_US
dc.title.alternativeProcedeu si instalatie de fabricare a diparatolil tricloretanului-
dc.typePatentsen_US
item.fulltextWith Fulltext-
item.cerifentitytypePublications-
item.grantfulltextreserved-
item.openairecristypehttp://purl.org/coar/resource_type/c_18cf-
item.openairetypePatents-
item.languageiso639-1en_US-
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