Please use this identifier to cite or link to this item:
http://hdl.handle.net/123456789/870
DC Field | Value | Language |
---|---|---|
dc.contributor.author | Dorobantu, Maria | - |
dc.contributor.author | Zlota, Arie | - |
dc.contributor.author | Barca, Elena | - |
dc.date.accessioned | 2017-04-20T13:46:06Z | - |
dc.date.available | 2017-04-20T13:46:06Z | - |
dc.date.issued | 1982-11-30 | - |
dc.identifier.other | Patent no. RO 80441-A | - |
dc.identifier.uri | http://hdl.handle.net/123456789/870 | - |
dc.description | Patent Assignee Name(s) and Code(s): COMB PETROCH BORZES; INST EPURAREA APELOR REZ | en_US |
dc.description.abstract | Para-toluene-sulphonic acid is prepd. by using the residue from di-p-tolyl-trichloroethane prodn. which contains 60% H2SO4 and 27% toluene-sulphonic acid. The residue is treated with toluene in ratio 1 : 1 to 1 : 4 (1 :1 :8), with stirring and heating, at 84-140 (110-114) deg.C. Unreacted and excess toluene distil azeotropically with water. After sepg. the water toluene layers, the water is discharged from process. Toluene is recirculated. Re-fluxing is continued 5-24 hrs., when the sulpho-mass contains 1-6% H2SO4. After cooling to 50-100 (70) deg.C, the vacuum distn. of excess toluene is continued. The excess toluene is reused in process. The resulting sulpho-mass contains 85% p-toluene-sulphonic acid. | en_US |
dc.language.iso | en_US | en_US |
dc.subject | Para-toluene-sulphonic acid | en_US |
dc.subject | Preparation | en_US |
dc.title | Para-toluene-sulphonic acid prepn. by treating di:para-tolyl-tri:chloroethane prodn. residue, contg. sulphuric acid and toluene-sulphonic acid, with toluene | en_US |
dc.title.alternative | Procedeu si instalatie de fabricare a diparatolil tricloretanului | - |
dc.type | Patents | en_US |
item.fulltext | With Fulltext | - |
item.cerifentitytype | Publications | - |
item.grantfulltext | reserved | - |
item.openairecristype | http://purl.org/coar/resource_type/c_18cf | - |
item.openairetype | Patents | - |
item.languageiso639-1 | en_US | - |
Appears in Collections: | Patents |
Files in This Item:
File | Description | Size | Format | Existing users please |
---|---|---|---|---|
Documentatie~RO80441A.pdf | 25.34 kB | Adobe PDF | Request a copy | |
~RO80441A.pdf | 90.22 kB | Adobe PDF | Request a copy |
Google ScholarTM
Check
Items in DSpace are protected by copyright, with all rights reserved, unless otherwise indicated.